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Title: Odorant Identification And Measurement In Natural Gas By Gas Chromatography
Author: H. K. BISHOP,J. R. Bricarello
Source: American Gas Association 1985
Year Published: 1985
Abstract: San Diego Gas & Electrics (SDG&E) location at the end of a transcontinental gas system makes it particularly concerned about odorant concentration in our natural gas. To determine the odorant compounds, their abundance, and iheir distribution in our gas delivery system, the SDG&E Laboratory developed a methodology, found suitable commercial equipment, and instituted an analysis program. The analysis was done on a gas chromatograph equipped with a Hall detector run in the sulfur selective mode. Identification was accomplished by use of a dual injection technique that separates the sulfur compounds and the overlapping mercaptan- sulfide peaks. Quantification was accomplished using injections of a standard gas and comparing peak areas of the sulfur compounds against it.

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